Hot-Roll Fabrication of Anisotropic Nanograin Nd-Fe-B Magnet

Nd-Fe-B based magnets have the highest energy product among all permanent magnets, which is required for numerous clean energy technologies. For higher temperature applications (T > 150°C), additions of heavy rare earth elements (HREEs) such as Dy are required to maintain sufficient coercivity during operation. Additions of Dy are expensive. Thus, it is desirable to reduce the need for HREEs by reducing the grain size to the nanoscale, which increases the coercivity and decreases its temperature dependence. Here, we report a novel nanograin Nd-Fe-B magnet fabrication method that is continuous and inexpensive. The process uses mechanically milled Nd-Fe-B melt-spun flakes as feedstock powder that is packed into a metal vessel and then hot rolled to form a fully dense and highly textured strip magnet with tailored thicknesses, down to 800 µm. Finally, using this process, fully dense nanograin bulk magnets can be synthesized in minutes compared to the traditional multi-step processes that are typically low throughput.. Authors: Pan, Chaochao [Ames Laboratory (AMES), Ames, IA (United States). Critical Materials Institute (CMI); Iowa State Univ., Ames, IA (United States)]; Ouyang, Gaoyuan [Ames Laboratory (AMES), Ames, IA (United States). Critical Materials Institute (CMI)]; Tang, Wei [Ames Laboratory (AMES), Ames, IA (United States). Critical Materials Institute (CMI)]; Liu, Xubo [Ames Laboratory (AMES), Ames, IA (United States). Critical Materials Institute (CMI)]; Ott, Ryan [Ames Laboratory (AMES), Ames, IA (United States). Critical Materials Institute (CMI)]. DOE Contract: AC02-07CH11358; AC52-07NA27344. Subjects: 36 MATERIALS SCIENCE; 75 CONDENSED MATTER PHYSICS, SUPERCONDUCTIVITY AND SUPERFLUIDITY