Creep ductility limiting mechanisms in an additively manufactured Al-Ce-Ni-Mn-Zr alloy

Tensile creep response and cavitation damage evolution in an additively manufactured Al-7.5Ce-4.5Ni-0.4Mn-0.7Zr (wt%) alloy with peak-aging and overaging treatments were investigated in the 300–400 ºC range. Microstructural heterogeneity and its response to heat treatment and subsequent creep deformation were studied to understand the interplay between cavity formation, creep lifetime and ductility. Increasing the applied stress activated the nucleation of more cavities, an experimental observation that is well described using the vacancy accumulation model. Cavities nucleated prematurely due to localized plasticity in the denuded zones that formed at/near melt-pool or grain boundaries. Microstructure/deformation heterogeneity with consequent evolution of stress triaxiality, especially at lower stresses, causes accelerated cavitation, thus producing low creep ductility (∼ 0.2–2.4 %), compared to (∼12–21 %) ductility of the alloy measured by regular tensile tests at equivalent temperatures. A constrained diffusional cavity growth mechanism with continuous cavity nucleation during creep is established as the dominant mechanism, implying that cavitation involves vacancy diffusion, yet its growth rate is dictated by the minimum creep rate. In conclusion, the ductility-limiting creep and cavitation mechanisms discussed here provide new insight into the creep behavior of 3D-printed metallic alloys.. Authors: Rakhmonov, Jovid [Oak Ridge National Laboratory (ORNL), Oak Ridge, TN (United States)] (ORCID:0000000326224128); Rahman, Obaidullah [Oak Ridge National Laboratory (ORNL), Oak Ridge, TN (United States)] (ORCID:0000000277810840); Bahl, Sumit [Oak Ridge National Laboratory (ORNL), Oak Ridge, TN (United States)] (ORCID:0000000294715001); Ziabari, Amir Koushyar [Oak Ridge National Laboratory (ORNL), Oak Ridge, TN (United States)] (ORCID:000000034776457X); Plotkowski, Alex [Oak Ridge National Laboratory (ORNL), Oak Ridge, TN (United States)] (ORCID:0000000154718681). DOE Contract: AC05-00OR22725. Subjects: Additive manufacturing; Aluminum alloys; Cavitation; Creep; Microstructure